ICS5000+高壓離子色譜系統

　　ICS-5000+高壓離子色譜

　　Thermo Scientific Dionex ICS-5000+ HPIC高壓離子色譜：世界上首款毛細管高壓、“只加水”離子色譜系統。全新的模塊設計具有極大的靈活性、功能更全面，操作更簡便，其完美卓越的性能將色譜分析帶入一個新的更高境界，分辨率更佳，分析速度更快。通過毛細管系統以及分析系統整合組成的ICS-5000+高壓離子色譜系統，能應對未來潛在的挑戰以及高級應用，該系統提高了工作效率，擴展了工作能力、提高了色譜性能。

　　主要特點

　　ICS-5000+具有出色的耐壓性能，兼容4μm離子色譜柱，極大提升了峰容量，進一步優化了分辨率。支持小粒徑色譜柱分離，大大提高了分辨率，結合快速離子色譜柱，分析速度可提升2倍，實現高分辨率、超快速分析

　　綠色理念離子色譜：毛細管色譜模式下，淋洗液發生器可以連續使用18個月，一年僅消耗5.25 L水，極大降低了試劑的消耗。時刻待機功能可節省大量時間，極大提高了分析效率，降低了實驗室的日常消耗

　　兼容毛細管、微孔和標準體系，色譜分析更加靈活

　　單系統和雙系統的靈活性配置，支持多種檢測器。輕松實現多種聯用技術——IC×IC (2D-IC)、IC-MS、IC-MS/MS和IC-ICP/MS。支持多通道、多檢測方式，支持多維色譜，具有更高的靈敏度

　　世界第一臺集生物液相、氨基酸分析、糖分析、反相液相色譜等功能于一身的離子色譜，可完成糖類、氨基酸、抗生素、小分子藥物、核酸以及蛋白質、多肽等的分離測定。電導檢測器、脈沖積分安培檢測器、紫外檢測器、熒光檢測器、CAD檢測器、熒光檢測器、質譜檢測器自由配置

　　挑戰分離極限

　　ICS-5000+ HPIC高壓毛細管離子色譜系統采用小粒徑的色譜柱(比如4 μm)，在不增加分析時間的情況下提高了色譜分辨率。

　　? 超強的耐高壓能力，支持小內徑、標準長度(250mm)的色譜柱

　　? 高效的色譜分辨率，提高了復雜樣品分析的準確性

　　? 分離效果，超乎想象——在不增加分析時間的情況下，可以分離出先前難以分離的峰

　　通過優化色譜柱內徑，支持高流速縮短分析時間，同時保持高分辨率。快速離子色譜柱有著較短的長度、較大的耐壓性能和較小粒徑的填料等特點，其分析速度要比常規色譜柱快2倍。

　　? 快速分離，增加樣品通量

　　? 提高分析效率

　　? 緊急樣品的快速結果篩查

　　系統特性：

　　?泵耐壓高達6000 psi

　　? 支持多通道分離，兼容毛細管體系，時刻待機，隨時進樣

　　? 采用標準型或微孔型色譜柱進行第一維色譜分析，毛細管柱進行第二維分析，獲取質譜級檢出限

　　? 支持包括電導、電化學、紫外可見光吸收、質譜在內的多種檢測技術

　　? 解放您的雙手——利用去離子水在線電解產生精確濃度的淋洗液

　　? 顏色標記式管路，人性化設計

　　? 降低使用成本：您可以安排更多時間從事其他重要工作，提高生產率

　　? 新型PdH參比電極，重現性極佳，保證不同時間、不同操作者和不同實驗室之間結果的一致性

　　? “譜立方”組件，預裝式設計，“零”死體積，組件易于配置，具有單獨控溫區

　　AS-DV全自動樣品處理系統

　　精密機械加工，重現性高

　　支持樣品在線過濾等樣品前處理功能

　　隨機取樣和重疊進樣功能

　　AS-AP全自動智能樣品處理系統

　　支持滿環、非滿環、毛細管模式和微量樣品進樣

　　具備自動樣品震蕩“AutoTrayShake”及“Puncture Offset”穿刺側移功能

　　全自動在線樣品制備(稀釋、預濃縮、基體消除、柱前衍生)

　　對熱不穩定樣品可進行溫度控制

　　支持在線監測電導和pH功能，智能判斷進樣與否

　　色譜數據系統

　　Chromeleon® 7.1變色龍軟件是蜚聲全球的色譜管理軟件，也是世界上zei早實現智能化、人性化、安全性、審計追蹤及電子簽名的軟件之一。變色龍軟件充分適應操作者windows的操作習慣，利用鼠標拖拽等進行程序編輯。變色龍軟件是世界上屈指可數的全面色譜管理系統，能夠雙向控制來自30多家公司的近300種離子、液相和氣相色譜系統及相關部件。

　　D-Library數據庫：通過搜索數據庫，您可及時分享國外zei新分析成果。

壓力范圍：

       分析： 0–35 MPa (0–5000 psi)

       毛細管：0–41 MPa (0–6000 psi)

流量范圍：

       分析：0.000-10.000 mL / min的流量，增量可設置在0.001mL / min，無需改變泵頭

       毛細管：0.001-0.100mL / min的流量，增量可設置在0.0001mL / min，典型的工作范圍為5-30μL / min的流量增量

流量準確度：< 0.1%

流量精度：< 0.1%

壓力波動：<1%(1.0mL / min)

真空脫氣(分析和毛細管)：集成，可選1元泵通道或4通道四元泵

活塞密封清洗：標準，自動操作

RFIC-EG梯度

         分析：0.1-100mM

        毛細管：0.1-200mM

梯度配比準確度和精密度(分析)：±0.5，在2mL / min

尺寸：41×23×56厘米(16×8.75×21.5英寸)

重量SP：20.4公斤(45磅) - DP：24.1(55磅)

更多參數：

Dionex iCS-5000+ 單泵和雙泵指標

泵

類型

串聯雙活塞泵，微處理器控制，穩定沖程，可變流速，具有專利技術的等動力淋洗液預混功能，無需使用阻尼器

結構

泵頭及所以接觸淋洗液的部件均采用具有化學惰性的PEEK材質，可兼容反相有機溶劑及pH 0-14的溶液

耐壓范圍：

0–35 MPa (0–5000 psi) (分析型)

0–41 MPa (0-6000 psi) (毛細管型)

流速范圍：

分析型：0.000–10.000 mL/min，增幅0.001 mL/min

毛細管型：0.001–0.100 mL/min，zei高可達3.000 mL/min，增幅0.0001 mL/min

流速精度：<0.1%

流速準確度：<0.1%

壓力波動：<1% (分析型)；<0.2% (毛細管型，帶阻尼器)在10 &micro;L/min, < 1.0% (無阻尼器)典型

加壓：無需加壓

真空脫氣：內置真空脫氣，單通道(等度泵)或四通道(四元梯度泵)

活塞密封清洗：標準配置，自動運行

梯度產生方式：四元低壓梯度或電解淋洗液在線產生高壓梯度

梯度類型：可產生線性、非線性、拋物線等多種形式的梯度

梯度比例精度和準確度：±0.5%

梯度混合：主動梯度混合器(選配)

Pump泵

Type Dual-piston (in series), microprocessor controlled, constant stroke, variable speed, patented Isokinetic Eluent Precompression 

Construction  Chemically inert, metal-free PEEK pump heads and flow path; compatible with aqueous eluents from pH 0–14 and reversed-phase solvents 

Pressure Range  Analytical: 0–35 MPa (0–5000 psi)

                         Capillary: 0–41 MPa (0–6000 psi)

Flow Rate Range  

Analytical: 0.000–10.000 mL/min with settable flow increments at 0.001 mL/min, without changing pump heads 

Capillary: 0.001–0.100 mL/min flow rate and up to 3.000 mL/min for pump priming mL/min with settable flow increments at 0.0001 mL/min, typical working range of 5–30 &micro;L/min

Flow Rate Precision (Analytical and Capillary)   < 0.1%  

Flow Rate Accuracy  < 0.1% 

Pressure Ripple  < 1% at 1.0 mL/min/typical, < 0.2% (with damper) at 10 &micro;L/min, < 1.0% (without damper) typical

Pressure  None required 

Vacuum Degasser (Analytical and Capillary)     Integrated, optional 1 channel for isocratic pump or 4 channel for quaternary pump

Piston Seal Wash Standard, automatic operation

Gradient Formation (Analytical and Capillary)   Quaternary low pressure (analytical only) or electrolytic eluent generation at high pressure 

RFIC-EG梯度：

• 分析：0.1–100 mM

• 毛細管：0.1–200 mM

• 梯度疲憊準確度：±0.5 at 2 mL/min

RFIC-EG Gradients

• Analytical: 0.1–100 mM 

• Capillary: 0.1–200 mM

• Gradient Profiles Any combination of an unlimited number of linear, convex, and concave positive and negative gradient profiles

• Gradient Proportioning Accuracy ±0.5 at 2 mL/min

• and Precision (Analytical Only)

• Gradient Mixing (Analytical Only) Passive mixers for 2 mm and 4 mm i.d. columns, optional

• Eluent Generation (Analytical and Capillary)     Optional eluent generation (RFIC-EG)

• Eluent On/Off Valve Electrically actuated, standard

• Leak Sensor Optical, standard

System Software

• Software Chromeleon Chromatography Data System software, supports Microsoft &reg;  Windows &reg;  7, Windows 

• Vista &reg; , and Windows XP &reg;  operating systems

• Automated Procedure Wizards Standard feature

• System Smart Startup and Shutdown Standard feature

• Application Templates Standard feature

• Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, HPLC, and MS

• Customizable System Control Panels Standard feature

• Signal Channels Pump pressure

• Data Trending Plots All numerical device parameters

• System Status Virtual Channels Standard feature

• Power Failure Protection Standard feature

• System Trigger Commands and Contitionals    Standard feature

• Daily Audit Trail Standard feature

• Sample Audit Trail Standard feature

• System Calibration Storage Factory, present and previous. Completely user selectable

• Customized Reporting Standard feature with unlimited report workbooks

• GLP Compliance Optional

Physical Specifications

• Power Requirements 90–265 V ac, 47–63 Hz

• Dimensions (h  × w  × d) 41 × 23 × 56 cm (16 × 8.75 × 21.5 in.)

• Weight SP: 20.4 kg (45 lb) — DP: 24.1 (55 lb)

• Flow Path: All polymeric (PEEK), anion or cation configuration11

EG淋洗液自動發生裝置

• zei小和zei大分析：0.1–100 mM

• 淋洗液濃度范圍毛細管：0.01-200mM

• 流速范圍：分析0.0–3.000 mL/min；毛細管：0.001–0.030 mL/min

• 淋洗液類型：分析: KOH, LiOH, NaOH; Carbonate; Carbonate/Bicarbonate; MSA 
                    毛細管: KOH, MSA

• zei大操作壓力：分析: Dionex EGC III: 21 MPa (3000 psi); Dionex EGC 500: 35 MPa (5000 psi)
                        毛細管: 35 MPa (5000 psi)

• 有機物zei大濃度：陽離子：不允許有有機溶劑存在；陰離子：能耐受25%的甲醇

• 淋洗液罐的數量：支持兩個淋洗液罐的同時使用

• 電源條件：90–265 V ac, 47–63 Hz

• 尺寸(h×w×d) ：41×23 ×56 cm(16×8.75×21.5in.)

• 重量：25 kg(40 lb)(不帶選配件下)

Dionex iCS-5000+ eg eluent generator  specifications

Minimum and Maximum Analytical: 0.1–100 mM

Eluent Concentration Capillary: 0.1–200 mM 

Flow Rates  Analytical: 0.1–3.000 mL/min；Capillary: 0.001–0.030 mL/min 

Eluent Types  

Analytical: KOH, LiOH, NaOH; Carbonate; Carbonate/Bicarbonate; MSA 

Capillary: KOH, MSA

Maximum Operating Pressure  

       Analytical: Dionex EGC III: 21 MPa (3000 psi); Dionex EGC 500: 35 MPa (5000 psi)

       Capillary: 35 MPa (5000 psi)

Maximum Solvent Concentration Cations: None

(Analytical and Capillary)  Anions: 25% methanol (KOH, NaOH and LiOH cartridges); None (Carbonate cartridge and EPM)

Gradient Profiles Standard - any combination of an unlimited number of linear, convex and concave positive and negative gradient profiles

Number of Cartridges Supported Two–dual cartridge support

RFIC Eluent Degasser (Analytical only)

Eluent degasser housed in the EG Module

System Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, 

and Windows XP operating systems

Automated Procedure Wizards Standard feature

System Smart Startup and Shutdown Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, 

HPLC, and MS

Customizable System Control Panels Standard feature

Signal Channels Eluent concentration

Data Trending Plots Device numerical parameters plotted

System Status Virtual Channels Standard feature

Power Failure Protection Standard feature

System Trigger Commands and Contitionals    Standard feature

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

Eluent Cartridge  Information Storage Serial number and expiration date

Customized Reporting Standard feature with unlimited report workbooks

GLP Compliance Optional package provides security, modification history, and electronic signatures

Physical Specifications

Power Requirements 90–265 V ac, 47–63 Hz

Dimensions (h  × w  × d) 41 × 23 × 56 cm (16 × 8.75 × 21.5 in.)

Weight 25 kg (40 lb) without optional items

Flow Path All polymeric (PEEK), anion or cation configuration

Dionex iCS-5000+ er eluent regeneration SPeCifiCationS (analytiCal)

Eluents Carbonate and carbonate/bicarbonate combinations up to 20 mM 

MSA up to 34 mM 

Flow Rates  1.00–2.00 mL/min

Continuous Operation with 4 L of Eluent Up to 28 days or 2000 samples, typically

Always on, Always Ready Capable Standard feature

Remains Fully Calibrated for Extended Standard feature, results are traceable to a single calibration

Periods of Time (≤ 28 Days):

System Wellness Consumables usage monitoring for predictive maintenance

Maximum Operating Pressure 21 MPa (3000 psi)

Operating Temperature Range 4–40 °C

Dionex iCS-5000+ DC DeteCtor/ChromatograPhy ComPartment SPeCifiCationS

Dual Temperature Zone Model Upper Zone Temp. Range: 10–40 °C (minimum temperature: ambient -15 °C); 

(maximum temperature: ambient +20 °C) 

Lower Zone Temp. Range: 10–70 °C (minimum temperature: ambient -15 °C)

(maximum temperature: ambient +50 °C)

Temperature Accuracy: ±0.5 °C

Temperature Stability: ±0.2 °C

Temperature Precision: ±0.2 °C

Lower Zone (Analytical)  Injection Valves: Up to two high-pressure valves,either 6- or 10-port, 2-position

Low Pressure Valves: Up to 2 inert, 2- or 3-way

Reaction Coil Heater (RCH): Holds two reaction coils

RCH Temperature Range: 5 °C above upper zone, 80 °C maximum 

AutoPrep Kit: Dual loop for sample preconcentration 

All valves and heater upgradable and field installable 

Automation Manager    Injection Valves: Up to two high-pressure valves, either 6- or 10-port, 2-position

(Optional - Analytical Only) Low Pressure Valves: Up to 2 inert, 2- or 3-way

Reaction Coil Heater (RCH): Holds two reaction coils

RCH Temperature Range: 5 °C above upper zone, 80 °C maximum 

AutoPrep Kit: Dual loop for sample preconcentration 

All valves and heater upgradable and field installable

Capillary IC Cube  One or two IC Cube modules holding the following:

(Optional - but required for Injection Valves: Up to two (one per cube) high-pressure valves, 4-port, 2-position. An optional capillary chemistries) 6-port, 2-position valve is available to support large loop and concentrator applications

EG Degasser 

Column and Guard

Carbonate Removal Device

Capillary Suppressor (See Suppressor section)

IC Cubes and cartridges are customer installable with pre-formed tubing and color-coded labeling

Capillary column heater 15 to 85 °C)

Flow Path Plumbing configurations for 4 mm, 2 mm, and 0.4 mm columns, fully inert, PEEK 

Detectors Any combination of two conductivity or electrochemical detectors, upgradeable and field installable. 

Dual detectors can be operated simultaneously or independently. Optional remote operation up to 3 m from instrument.

Analog Signal Output Two analog output channels, two 24 V relays, 2 TTL Out and 8 TTL In lines, upgradable and field installable, optional Leak Detection Optical leak sensor standard

Application Control Automation Standard. All DC modules come equipped with two switched AC controllers built-in to automate external devices and the ability to control up to six low pressure 2-way or 3-way valves for fluidic automation

Suppression

Non-Suppressed Conductivity Supported - both anion and cation

Suppressor Wear Parts None. No valves, pumps, peristaltic pump tubing, or inline filters required

Chemical Suppression 2 mm and 4 mm anion and cation membrane suppression available

Displacement Chemical Suppression 2 mm and 4 mm anion and cation membrane suppression available

Electrolytic Suppression, Self-Regenerating     0.4 mm (with optional IC Cube) 2 mm and 4 mm anion and cation. Membrane and MonoDisc 

suppression bed types available. Membrane for capillary (0.4 mm) suppressor

Electrolytic Suppression, Self-Regenerating,    0.4 mm (with optional IC Cube) 2 mm and 4 mm anion and cation. Membrane and MonoDisc 

External Water Mode suppression bed types available for 4 mm and 2 mm. Membrane for capillary (0.4 mm) suppressor Salt Converter Available in 2 and 4 mm versions

Dionex AMMS-ICE Available in 9 mm version

Carbonic Acid Removal for Anions Thermo Scientific Dionex ASRS &trade;  300 or Dionex AMMS &trade;  300 plus Dionex CRD 200 and 

CRD 300 for 2 and 4 mm versions, Dionex ACES &trade;  300 plus Dionex CRD 200 (0.4 mm) for capillary suppressors13

Dionex iCS-5000+ DC DeteCtor/ChromatograPhy ComPartment SPeCifiCationS  (CONTINUED)

Suppressors

Suppression Capacities Dionex ASRS 300 (4 mm): 200 μeq/min

Thermo Scientific Dionex CSRS &trade;  300 (4 mm): 110 μeq/min

Dionex ASRS 300 (2 mm): 50 μeq/min

Dionex CSRS 300 (2 mm): 37.5 μeq/min

Dionex AMMS 300 (4 mm): 150 μeq/min

Thermo Scientific Dionex CMMS &trade;  300 (4 mm): 150 μeq/min

Dionex AMMS 300 (2 mm): 37.5 μeq/min

Dionex CMMS 300 (2 mm): 37.5 μeq/min

Dionex AAES: 25 μeq/min

Dionex CAES: 25 μeq/min

Dionex AMMS-ICE 300: N/A

Dionex ACES 300 (0.4 mm): 2 &micro;eq/min

Thermo Scientific Dionex CCES &trade;  300 (0.4 mm): 1.5 &micro;eq/min

Suppressor Void Volumes Dionex SRS 300 (4 mm): < 50 μL

Dionex SRS 300 (2 mm): < 15 μL

Dionex MMS 300 (4 mm): < 50 μL

Dionex MMS 300 (2 mm): < 15 μL

Dionex AMMS-ICE 300 (4 mm): < 50 μL

Dionex AES (Anion or Cation): < 35 μL

Dionex ACES 300 (0.4 mm): < 1.0 &micro;L

Dionex CCES 300 (0.4 mm): < 1.0 &micro;L

System Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, 

and Windows XP operating systems

Automated Procedure Wizards 2 mm and 4 mm anion and cation membrane suppression available

Electrolytic Suppression, Self-Regenerating     Standard feature

System Smart Startup and Shutdown Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, HPLC, and MS 

Customizable System Control Panels Standard feature

Signal Channels Detector signals, detector background signals, temperatures

Data Trending Plots All device numerical parameters plotted

System Status Virtual Channels Standard feature

Power Failure Protection Standard feature

System Trigger Commands and Conditionals   Standard feature

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

System Calibration Storage Factory, present, and previous. Completely user selectable

GLP Compliance Optional

Physical Specifications

Power Requirements 90–265 V ac, 47–63 Hz; (auto-sensing power supply; no manual voltage or frequency 

adjustment required)

Dimensions (h  × w  × d) 44.5 × 42 × 57 cm (17.5 × 16.5 × 22.5 in.)

Weight 38 kg (84 lb) 

Flow Path All polymeric (PEEK), anion or cation configuration14

Dionex iCS-5000+ CD ConDuCtiVity DeteCtor SPeCifiCationS

Electronics Type Microprocessor controlled digital signal processing, autoranging

Cell Drive  8 kHz square wave

Linearity    1%

Resolution  0.00238 nS/cm

Flow Path Plumbing configurations for 4 mm, 2 mm, and 0.4 mm columns, fully inert, PEEK 

Output Range Digital Signal Range: 0–15,000 &micro;S/cm

Analog Signal Range: 0–15,000 &micro;S/cm

Noise, Wet < 0.2 nS at 23 &micro;S/cm background

< 0.1 nS at 1 &micro;S/cm background

Filter Rise times 0 to 10 s, programmable

Sample Rate 1 to 100 Hz, user settable or automatic

Cell Temperature 5 °C above DC upper zone temperature to 60 °C maximum. User settable, working range is

identical to settable range.

Cell Temperature Stability < 0.001 °C

Cell Temperature Compensation Default 1.7% per °C; programmable from 0–3% per °C

Flow Cell Maximum Pressure 10 MPa (1500 psi)

Flow Cell Volume Analytical: 0.7 &micro;L

Capillary: 0.02 &micro;L

Cell Electrodes Passivated 316 stainless steel. Compatible with MSA

Cell Body Chemically inert polymeric material

Heat Exchanger Inert, tortuous-path for low axial dispersion

Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, 

and Windows XP operating systems

Automated Procedure Wizards Standard feature

System Smart Startup and Shutdown Standard feature

System Wellness and Predictive Performance  Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, 

HPLC, and MS 

Customizable System Control Panels Standard feature

Signal Channels Conductivity, Total Conductivity

Data Trending Plots Detector numerical parameters plotted 

System Status Virtual Channels Standard feature

Power Failure Protection Standard feature

System Trigger Commands  Standard feature and Conditionals

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

System Calibration Storage Factory, present, and previous. Completely user selectable.

Customized Reporting Standard feature with unlimited report workbooks

GLP Compliance Optional

Physical Specifications

Dimensions (h  × w  × d) 6.9 × 16.7 × 9.9 cm (2.7 × 6.5 × 3.9 in.)

Weight 400 g (1.6 lb) 15

Dionex iCS-5000+ eD eleCtroChemiCal DeteCtor SPeCifiCationS

Electronics Type Microprocessor controlled digital signal processing

Electronic Noise (Wet Noise) IPAD (Au electrode) < 50 pC at 10 mM KOH, DC Amperometry (GC) < 10 pA at catecholamine eluent

(Analytical and Capillary)

Potential Range -2.0 to 2.0 V in 0.001 V increments

Signal Range (Digital and Analog) Integrated Amperometry: 50 pC to 200 &micro;C

DC Amperometry: 5 pA to 74 &micro;A

Filter 0–10 s response time, user settable

Control Mode Local or remote control using relay closures or TTL, or control using Chromeleon software via DC module

Cell Body Titanium body with narrow-bore PEEK inlet tubing for capillary format, titanium inlet tubing for analytical format. Compatible with 0.2–0.6 mm i.d. columns (PEEK inlet), 2–7 mm i.d. columns (Ti inlet)

Working Electrodes Conventional: gold, glassy carbon, platinum, and silver

Disposable: gold, platinum, carbon, and silver

Reference Electrode pH-Ag/AgCl combination, one piece design (Analytical and Capillary) 

PdH, one piece design (Capillary Only)

Autoranging  Yes

Analog Output User selectable full scale of 10, 100, or 1000 mV

Cell Volume at Working Electrode < 0.2 &micro;L

Maximum Cell Operating Pressure 0.7 MPa (100 psi)

Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, and Windows XP operating systems

Detection Modes DC amperometry, pulsed amperometry, and integrated amperometry. Detection modes include use 

of multiple waveforms and multiple integration times to optimize detection conditions for individual 

analytes. Integrated amperometry mode—unlimited changes to the waveform profile&rsquo;s number of segments, duration of each segment, and voltage applied at each segment.

3D Amperometry  Three-dimensional display of the raw integrated amperometry data set, with crosshairs on an (Chromeleon 6.8 software only) isoamperometric plot used to select slices of the plot along the applied voltage axis (to render a chromatogram) and along the time axis (to render a voltammogram).

Automated Procedure Wizards Standard feature

System Smart Startup and Shutdown Standard feature

System Wellness and Predictive Performance  Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, HPLC, and MS

Customizable System Control Panels Standard feature

Signal Channels Electrochemical and total electrochemical signals

Data Trending Plots All detector numerical parameters plotted

System Status Virtual Channels Standard feature

Power Failure Protection Standard feature

System Trigger Commands Standard feature and Conditionals

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

System Calibration Storage Factory, present, and previous. Completely user selectable.

Customized Reporting Standard feature with unlimited report workbooks

GLP Compliance Optional

Physical Specifications

Dimensions (h  × w  × d) 6.9 × 16.7 × 9.9 cm (2.7 × 6.5 × 3.9 in.)

Weight 400 g (1.6 lb) 16

Dionex iCS-SerieS PDa PhotoDioDe array specifications

Optics

Photodiode Array 1024 element

Pixel Resolution 0.7 nm

Lamps Tungsten and deuterium

Optical Resolution 1.0 nm

Wavelength Range 190–800 nm

Electronics

Analog Outputs Four, 0–3 AU, 1000 mV range

Control Modes Software remote control through Chromeleon software

Flow Cell 

Standard PEEK or SST, 13 &micro;L, 10 mm path length

Semi-Prep PEEK, 0.7 &micro;L, 0.4 mm path length

Maximum Flow Operating Pressure 300 psi (< 2 MPa) PEEK

500 psi (< 3 MPa) SST

Performance

Noise ±10 &micro;AU at 254 nm (flowing water, 2s rise time)

±15 &micro;AU at 520 nm (flowing water, 2s rise time)

Drift < 500 &micro;AU/h

Wavelength Accuracy ±1 nm, self-calibration with deuterium lines, verification with built-in holmium oxide filter

Linearity > 2 AU

Physical Specifications

Power Requirements 90–265 V ac, 47–63 Hz

Operating Temperature Range 4–40 °C (40–104 °F)

Operating Humidity Range 5–95% relative, noncondensing

Dimensions (h  × w  × d) 17.4 × 44.4 × 50.3 cm (6.8 × 17.5 × 19.8 in.)

Weight 18.1 kg (40 lb)

tC thermal ComPartment moDule SPeCifiCationS (analytiCal)

Temperature Range 5–85 °C (max 18 °C below ambient) in 0.1 °C increments

Temperature Performance Accuracy: ± 0.5 °C

Stability:  ± 0.1 °C

Precision:  ± 0.1 °C

Heat up / Cool down Time Typically 15 minutes - 20 °C to 50 °C and 50 °C to 20 °C

High-Pressure Valve Types Six-port/two position - Rheodyne PEEK (injection) valve

Ten-port/two position - Rheodyne PEEK (switching) valve

Column Capacity Three column sets, 1–9 mm

Maximum Column Length 300 mm + 50 mm guard column

Precolumn Heat Exchangers (optional) Two low delay volume exchangers

General Specifications

Standard Chromeleon software

Computer Connection USB

Leak Detection Humidity and vapor sensors

TTL and Relay inputs and outputs Two digital inputs/outputs, two relay outputs

Physical Specifications

Power Requirements 90–265 V ac, 47–63 Hz

Operating Temperature Range 4–40 °C (40–104 °F)

Operating Humidity Range 5–95% relative, noncondensing

Dimensions (h  × w  × d) 17.4 × 44.4 × 50.3 cm (6.8 × 17.5 × 19.8 in.)

Weight 15.4 kg (34 lb)17

Dionex iCS-SerieS Variable waVelength DeteCtor SPeCifiCationS

Optics

Optical System Dual beam forward optics design (monochromator) single or multiple (4-channel) wavelength UV-vis 

detector options 

Light Source Deuterium lamp for UV range; tungsten lamp for visible range

Wavelength Range 190 to 900 nm in 1 nm increments

Electronics

Analog Output Ranges (optional) 0.001–3.0 AU

Rise Time 0.00–4.55 s

Full-Scale Recorder Output 1 V or 10 V

Data Collection rate up to Full dynamic autoranging digital absorbance signal output to Chromeleon software

100 Hz Digital Output

Control Modes Software remote control through Chromeleon software

Flow Cells

Cell PEEK

Cell Path Length 10 mm (Standard and Capillary), 7 mm (Micro)

Cell Volume 11 &micro;L (Standard) 2.5 μL (Micro) 0.18 μL (Capillary)

Heat Exchanger Volume 8.8 &micro;L

Maximum Flow Cell Operating Pressure 725 psi (5 MPa)

Performance

Wavelength Accuracy ±1 nm

Linearity > 2 AU

Bandwidth  6 nm at 254 nm

Noise Typically - < ±2.5 × &micro;AU at 254 nm

Drift < 0.1 m &micro;AU/h at 254 nm

Physical Specifications

Power Requirements 85–265 V ac, 47–63 Hz

Operating Temperature Range 10–35 °C (50–95 °F)

Operating Humidity Range 5–80% relative, noncondensing

Dimensions (h  × w  × d) 15.2 × 44.4 × 50.3 cm (6.0 × 17.5 × 19.8 in.)

Weight 15.4 kg (34 lb)18

Dionex aS-aP autoSamPler SPeCifiCationS

Sample Capacity 10 mL vials: 81

1.5 mL vials: 120

0.3 mL vials: 120

Well Plates: 288 (3 × 96 standard or deep well)

Well Plates: 1152 (3 × 384 standard well) 

Minimum Sample Volume 10 &micro;L can be sampled from a 300 &micro;L microvial; 20 &micro;L can be sampled from a 500 &micro;L microvial

Maximum Injection Volume 7500 &micro;L

Variable Volume Range 1–100 &micro;L in 0.1 &micro;L increments; 100–7500 &micro;L in 1 &micro;L increments

Injection Cycle Time (including sample 15 s with sample overlap function; 30 s for a 5 &micro;L full loop without sample overlap

   prep such as dilution)

Injection Modes Full Loop; Partial Loop; Limited Sample; Capillary

Sampling Technique Pull Mode; Push Mode

Injection Precision Fixed Loop: < 0.3% RSD at 20 &micro;L; Partial Loop: < 0.5% RSD at 20 &micro;L

Capillary Mode: < 0.5% RSD at 0.4 &micro;L

Dilution 1:1 to 1:1000

AutoDilution With post-run functionality and Chromeleon AutoDilution License

Dilution Precision < 1.0% RSD for a 1:10 dilution

Carryover < 0.01% with 500 &micro;L flush volume

Sample Tray Thermostatting 4 °C to 60 °C, optional

Sample Conductivity and pH Inline measurement of sample conductivity and pH with postrun functionality, optional

Dual Instrument Support Sequential (asynchronous) and Simultaneous modes, field upgradeable, optional

Sample Degassing CRD 200/300, upgradeable, user installable

Injection Valves One or two 2-position, 6- or 10-port

Diverter Valve One 2-position, 6- or 10-port

Sample Preparation Dilution, addition of internal standards, concentration/matrix elimination, derivatization, etc.

Inline Sample Filtration Dual filter, backflush, optional

Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, 

and Windows XP operating systems

Automated Procedure Wizards Standard feature

System Smart Startup and Shutdown Standard feature

System Wellness and Predictive Performance  Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, HPLC, and MS

Customizable System Control Panels Standard feature

Power Failure Protection Standard feature

System Trigger Commands Standard feature and Conditionals

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

System Calibration Storage Factory, present, and previous. Completely user selectable.

Customized Reporting Standard feature with unlimited report workbooks

GLP Compliance Optional

Physical Specifications

Dimensions (h  × w  × d) 44.5 × 35.9 × 51.6 cm (17.5 × 14.1 × 20.3 in.)

Weight < 25.2 kg (< 55.5 lb)

< 26.8 kg (< 59.0 lb) with sample temperature control

Power 90–265 V ac, 47–63 Hz

Flow Path All polymeric (PEEK), anion or cation configurations